HRID980424

反应详情

EQUATION

反应方程式

HRID 980424 的结构方程式

PROCEDURE

实验过程

For conversion into the acid chloride, trans-4-pentylcyclohexylacetic acid (12.0 g, 0.0566 mol) was reacted for about 1 hour on an oil bath at 80° C. with thionyl chloride (50 ml). The solution obtained was evaporated under reduced pressure, treated with absolute toluene (50 ml) and once more evaporated under reduced pressure.

WORKUP

后处理

  1. customThe solution obtained
  2. customwas evaporated under reduced pressure
  3. additiontreated with absolute toluene (50 ml)
  4. customonce more evaporated under reduced pressure