化工社化工社 化学情報印刷レポート · 研究参考用
Thionyl Chloride → HCID 178444488、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | HCID 178444491 | HCID 178444491 | — |
| 生成物 | HCID 178444488 | HCID 178444488 | — |
反応手順
For conversion into the acid chloride, trans-4-pentylcyclohexylacetic acid (12.0 g, 0.0566 mol) was reacted for about 1 hour on an oil bath at 80° C. with thionyl chloride (50 ml). The solution obtained was evaporated under reduced pressure, treated with absolute toluene (50 ml) and once more evaporated under reduced pressure.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04637897 |
| 出典データセット | uspto-grants-1987_01 |
| ORD ID | ord-f5c682759cb14903a7140f0f7b826a0a |
| 出典メモ | uspto-grants-1987_01 |