1-Butanol → Phenylacetone

HRID 980586Notes

Reaction equation

HRID 980586 reaction equation
N([O:3][CH2:4][CH2:5][CH2:6][CH3:7])=O.[CH2:8](O)[CH2:9][CH2:10][CH3:11].N(O[CH3:16])=O>CO>[C:6]1([CH2:5][C:4](=[O:3])[CH3:16])[CH:7]=[CH:11][CH:10]=[CH:9][CH:8]=1

Participants

5

Reactant 3

HCID 2631-ButanolHCID 10996Butyl nitriteHCID 12231Methyl nitrite

Product 1

HCID 7678Phenylacetone

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Phenylacetone was prepared in the same manner as in Example 1, except that n-butyl nitrite and n-butyl alcohol were used in lieu of methyl nitrite and methyl alcohol and that the reaction temperature was changed to 55° C.

Workup

  1. customwas changed to 55° C.

Sources & evidence

ORD record
ord-2de6c4227ecf483ea3a18cbb9fcfaec3
Source dataset
uspto-grants-1987_01
Patent number
US04638094

Reaction notes

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