Sodium Hydroxide → Sodium trifluoromethanesulfonate

HRID 980782Notes

Reaction equation

HRID 980782 reaction equation
[F:1][C:2]([F:8])([F:7])[S:3]([OH:6])(=[O:5])=[O:4].[OH-].[Na+:10]>O>[F:1][C:2]([F:8])([F:7])[S:3]([O-:6])(=[O:5])=[O:4].[Na+:10]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 62406Trifluoromethanesulfonic acid2×

Product 1

HCID 23676748Sodium trifluoromethanesulfonate

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Trifluoromethanesulfonic acid (17.50 g) was placed in a graduated cylinder and diluted with water (30 ml). The trifluoromethanesulfonic acid was neutralized with 10% sodium hydroxide to a pH of 7.2. The solution was transferred to a rotary evaporator, evaporated to dryness and placed under a vacuum overnight (20.2 g). The sample was collected, ground to a fine powder in mortar and pestle and dried to a constant weight (19.18 g).

Workup

  1. customThe solution was transferred to a rotary evaporator
  2. customevaporated to dryness
  3. customplaced under a vacuum overnight (20.2 g)
  4. customThe sample was collected
  5. customground to a fine powder in mortar and pestle and dried to a constant weight (19.18 g)

Sources & evidence

ORD record
ord-906c03146b304485b607a4e130a52ee7
Source dataset
uspto-grants-1987_01
Patent number
US04639364

Reaction notes

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