HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Thiophenecarbonyl chloride → HCID 13228911, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Thiophenecarbonyl chloride | HCID 78928 | — |
| Reactant | Ici 109,081 | HCID 161928 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 13228911 | HCID 13228911 | 51.9% |
Reaction Steps
A mixture of 1.1 g of 2-thenoyl chloride, 1.0 g of 6-(p-aminophenyl)-5-methyl-4,5-dihydro-3(2H)-pyridazinone and 10 ml of benzene was treated in the same manner as described in Example 1 to effect reaction whereby 800 mg of the title compound was obtained. M.P. 256°-258° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04639451 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-ec37c800645942f980234c3e0c4de6af |
| Source note | uspto-grants-1987_01 |