HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyacetonitrile → HCID 12878154, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyacetonitrile | HCID 7857 | — |
| Reactant | Hexylamine | HCID 8102 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 12878154 | HCID 12878154 | — |
Reaction Steps
In a flask of 100 ml, 5.7 gr of hydroxyacetonitrile (0.1 mol) were mixed with 11 gr of hexylamine (0.11 mol) dissolved in 10 ml of MeOH. The temperature quickly raised during mixing. The solution was allowed to stand for 24 hours. The methanol was evaporated and the obtained liquid was distilled at 72° under 0.8 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04639468 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-9475fb1c7b9a40afae58ce4b66dfa890 |
| Source note | uspto-grants-1987_01 |