HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl fluorosulfate → HCID 20220803, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl fluorosulfate | HCID 9870 | — |
| Reactant | Methoxyacetyl chloride | HCID 96623 | — |
| Reactant | HCID 20220776 | HCID 20220776 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 20220803 | HCID 20220803 | — |
Reaction Steps
Following the procedure of Preparation 24, but using p-nitrobenzyl thioformylglycinate (254 mg.), magic methyl (81 μl.), triethylamine (350 μl) and methoxyacetyl chloride (91 μl.), there were obtained 26 mg of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04639441 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-a0c755fa9b6244549cab249d6f04017a |
| Source note | uspto-grants-1987_01 |