HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
8(5H)-Quinolinone, 5-[[4-(diethylamino)-2-methylphenyl]imino]-, (5Z)- → Indoaniline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 8(5H)-Quinolinone, 5-[[4-(diethylamino)-2-methylphenyl]imino]-, (5Z)- | HCID 364894 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | Indoaniline | HCID 24748760 | — |
Reaktionsschritte
Then, a solution prepared by dissolving 285.3 mg of Ni(ClO4)2.6H2O in 50 ml of water, was added under a nitrogen atmosphere to a solution prepared by dissolving 100 mg of 5-(2'-methyl-4'-diethylaminophenylimino)quinoline-8-one obtained above in 50 ml of 99% ethanol, and the mixture was stirred at room temperature for about 30 minutes. Formed precipitates were subjected to suction filtration, washed with water and dried to obtain a metal-containing indoaniline compound having the formula: ##STR9##
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04990433 |
| Quelldatensatz | uspto-grants-1991_02 |
| ORD ID | ord-d8d61d8ff3454d6b8cbc42e442683859 |
| Quellennotiz | uspto-grants-1991_02 |