HRID981010

反应详情

EQUATION

反应方程式

HRID 981010 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Then, a solution prepared by dissolving 285.3 mg of Ni(ClO4)2.6H2O in 50 ml of water, was added under a nitrogen atmosphere to a solution prepared by dissolving 100 mg of 5-(2'-methyl-4'-diethylaminophenylimino)quinoline-8-one obtained above in 50 ml of 99% ethanol, and the mixture was stirred at room temperature for about 30 minutes. Formed precipitates were subjected to suction filtration, washed with water and dried to obtain a metal-containing indoaniline compound having the formula: ##STR9##

WORKUP

后处理

  1. customThen, a solution prepared
  2. additionwas added under a nitrogen atmosphere to a solution
  3. customprepared
  4. customFormed
  5. customprecipitates
  6. filtrationwere subjected to suction filtration
  7. washwashed with water
  8. customdried