HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminum hydride → HCID 54279535, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminum hydride | HCID 14487 | — |
| Reactant | HCID 54568910 | HCID 54568910 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 54279535 | HCID 54279535 | 79% |
Reaction Steps
The same procedure as that described in example 2(b) was followed but using 5.92 g of 14-isopropyl-13,15-dioxabicyclo[10.3.0]pentadeca-4,8-diene and 39.5 ml of a 1.2M solution of DIBAH in toluene. 4.71 g of 12-isobutoxy-4,8-cyclododecadien-1-ol were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04990495 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-0872ad5591d04a3787cf507f02cde8e7 |
| Source note | uspto-grants-1991_02 |