HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 9321153, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | 5-Bromoisatin | HCID 6889 | — |
| Reactant | HCID 12198272 | HCID 12198272 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 9321153 | HCID 9321153 | — |
Reaction Steps
A solution of 2.26 g 5-bromoisatin (0.01 mole) and 1.36 g 2-amino N-methyl-p-toluidine (0.01 mole) in 15 ml acetic acid is boiled with reflux for 45 minutes. Finally hydrogen bromide is introduced and the mixture is boiled for further 2 hours. After cooling it is poured into water. The dried reaction product is recrystallized from acetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04990510 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-67f1013c7d0346239fa081c7ecfcada4 |
| Source note | uspto-grants-1991_02 |