HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 18329731, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Methyl Isobutyl Ketone | HCID 7909 | — |
| Reactant | 4-Iodophenol | HCID 10894 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Product | HCID 18329731 | HCID 18329731 | — |
Reaction Steps
A mixture of 4-iodophenol (1.0 g) 1-bromo-2-methoxyethane (0.7 g), potassium iodide (0.83 g), potassium carbonate (0.7 g) and methyl isobutylketone (10 ml) was refluxed for 18 h, diluted with ER (50 ml), filtered and evaporated. The residue was distilled to give the title compound (0.83 g). T.l.c. (cyclohexane-ER 1:1) Rf 0.6
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04990505 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-4588373aecbf45c290aab60b0b530111 |
| Source note | uspto-grants-1991_02 |