HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic anhydride → HCID 20071767, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic anhydride | HCID 9845 | — |
| Reactant | HCID 20071758 | HCID 20071758 | — |
| Product | HCID 20071767 | HCID 20071767 | — |
Reaction Steps
A solution of the sulfoxide from Step C of this Example (10 g) in trifluoroacetic anhydride (50 ml) was heated at 45° C. for 25 minutes and the mixture was evaporated, and then coevaporated with toluene, to dryness to give the title compound as an oil (15 g, crude) which was used directly in the following step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04990526 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-6676e588402743eda18ec160fd86ddfa |
| Source note | uspto-grants-1991_02 |