HRID981351

反应详情

EQUATION

反应方程式

HRID 981351 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 19.7 g. (0.1 mole) of bromosuccinic acid, 40.1 g. (0.2 mole) of tridecanol, 0.25 g. of p-toluenesulfonic acid and 200 ml. of toluene is refluxed for 7 hours, using a Dean-Stark trap. There is collected 3.6 ml. of H2O in the trap which is exactly the calculated amount for this reaction when completed.

WORKUP

后处理

  1. additionA mixture of 19.7 g
  2. customThere is collected 3.6 ml
  3. customfor this reaction when