HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20070371, compound → 1-Propanol, 2-[(2-aminophenyl)amino]-2-methyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20070371 | HCID 20070371 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-Propanol, 2-[(2-aminophenyl)amino]-2-methyl- | HCID 11961557 | 98% |
Reaction Steps
2-(1,1-dimethyl-2-hydroxyethyl)aminonitrobenzene (10 g) in ethanol (200 ml) was hydrogenated at 50p.s.i. (345 kPa) over 5% Pd/C (0.5 g) for 2 hours. The catalyst was filtered off and the solvent removed under reduced pressure yielding the title compound as a yellow foam 8.4 g (98%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04992447 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-cdeb9fdeb99742dfa3c8a0d9568cd911 |
| Source note | uspto-grants-1991_02 |