Furfurylamine → HCID 54499093, compound

HRID 981722Notes

Reaction equation

HRID 981722 reaction equation
[CH2:1]([NH2:7])[C:2]1[O:6][CH:5]=[CH:4][CH:3]=1.[CH2:8]([C:11]12[CH2:17][CH:14]([CH:15]=[CH:16]1)[CH2:13][CH:12]2[C:18](Cl)=[O:19])[CH:9]=[CH2:10]>>[CH2:1]([NH:7][C:18]([CH:12]1[CH2:13][CH:14]2[CH2:17][C:11]1([CH2:8][CH:9]=[CH2:10])[CH:16]=[CH:15]2)=[O:19])[C:2]1[O:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 3438FurfurylamineHCID 20070591HCID 20070591, compound

Product 1

HCID 54499093HCID 54499093, compound

Procedure

21.4 g of furfurylamine and 39.3 g of allylbicyclo[2.2.1]hept-5-ene-2-carbonyl chloride are reacted in accordance with process A, affording 38.1 g (73.8% of theory) of a reddish brown liquid resin; η25 =1287.2 m Pas.

Workup

  1. customaffording 38.1 g (73.8% of theory) of a reddish brown liquid resin

Sources & evidence

ORD record
ord-77f8182803734f579571cb73cff3fdf4
Source dataset
uspto-grants-1991_02
Patent number
US04992518

Reaction notes

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