Ethylenediamine → HCID 20071075, compound

HRID 981824Notes

Reaction equation

HRID 981824 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4](Cl)[C:3]=1[N+:9]([O-:11])=[O:10].[CH2:12]([NH2:15])[CH2:13][NH2:14]>>[ClH:1].[ClH:1].[NH2:14][CH2:13][CH2:12][NH:15][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([NH:14][CH2:13][CH2:12][NH2:15])[C:3]=1[N+:9]([O-:11])=[O:10]

Participants

3

Reactant 2

HCID 3301Ethylenediamine2×HCID 117591,3-Dichloro-2-nitrobenzene

Product 1

HCID 20071075HCID 20071075, compound

Procedure

0.16 mole (30 g) of 2,6-dichloronitrobenzene is added to 100 ml of ethylenediamine. The mixture is heated under reflux for 4 hours. The unreacted ethylene diamine is stripped off under vacuum. The expected product is precipitated by adding a 7N solution of hydrochloric acid to the residue obtained.

Workup

  1. temperatureThe mixture is heated
  2. temperatureunder reflux for 4 hours
  3. customThe expected product is precipitated
  4. additionby adding a 7N solution of hydrochloric acid to the residue
  5. customobtained

Sources & evidence

ORD record
ord-7f9ac3b8c0594bd6938a79c17d7b8cf8
Source dataset
uspto-grants-1991_02
Patent number
US04992586

Reaction notes

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