HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylenediamine → HCID 20071075, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | 1,3-Dichloro-2-nitrobenzene | HCID 11759 | — |
| Product | HCID 20071075 | HCID 20071075 | — |
Reaction Steps
0.16 mole (30 g) of 2,6-dichloronitrobenzene is added to 100 ml of ethylenediamine. The mixture is heated under reflux for 4 hours. The unreacted ethylene diamine is stripped off under vacuum. The expected product is precipitated by adding a 7N solution of hydrochloric acid to the residue obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04992586 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-7f9ac3b8c0594bd6938a79c17d7b8cf8 |
| Source note | uspto-grants-1991_02 |