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HRID981844

反应详情

EQUATION

反应方程式

HRID 981844 的结构方程式

REACTANTS

反应物

3
结构：CCOC(=O)CCc1ccccc1OC
HCID578401

Ethyl 3-(2-methoxyphenyl)propanoate

C12H16O3

结构：[Al+3].[Cl-].[Cl-].[Cl-]
HCID6451240

未命名化合物

结构：CCOC(=O)c1cccc(C(=O)O)c1.[Cl-]
HCID86744615

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)CCc1cc(C(=O)c2cccc(C(=O)OCC)c2)ccc1OC
HCID14739655

未命名化合物

收率 104.6%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

Following the procedure of Example 1, 30.6 g of isophthalic acid monoethyl ester monochloride and 30 g of ethyl 2-methoxybenzene propanoate were treated with 57 g of aluminum chloride in dichloromethane to provide 53.6 g of the desired title product, as an oil.