HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Pyridinecarboxaldehyde → 2-[(2,4-Dimethyl-3-nitrophenylimino)-methylene]-pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Pyridinecarboxaldehyde | HCID 14273 | — |
| Reactant | 2,4-Dimethyl-3-nitroaniline | HCID 13369963 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-[(2,4-Dimethyl-3-nitrophenylimino)-methylene]-pyridine | HCID 20068353 | — |
Reaction Steps
3.3 g of 4-amino-2-nitro-m-xylene and 2.1 g of 2-pyridinealdehyde were dissolved in 50 ml ethanol and left to stand. Crystals slowly precipitated and were filtered off under suction and washed with ethanol. The dried product (3.0 g) had a melting point of 114° to 116° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04994087 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-2e72d61591314d2f90044a849a2c797c |
| Source note | uspto-grants-1991_02 |