huagongshe.com
HRID981862

反应详情

EQUATION

反应方程式

HRID 981862 的结构方程式

REACTANTS

反应物

2
结构：O=Cc1ccccn1
HCID14273

2-Pyridinecarboxaldehyde

C6H5NO

结构：Cc1ccc(N)c(C)c1[N+](=O)[O-]
HCID13369963

未命名化合物

PRODUCTS

生成物

1
结构：Cc1ccc(N=C=C2C=CC=CN2)c(C)c1[N+](=O)[O-]
HCID20068353

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

3.3 g of 4-amino-2-nitro-m-xylene and 2.1 g of 2-pyridinealdehyde were dissolved in 50 ml ethanol and left to stand. Crystals slowly precipitated and were filtered off under suction and washed with ethanol. The dried product (3.0 g) had a melting point of 114° to 116° C.

WORKUP

后处理

  1. waitleft
  2. customCrystals slowly precipitated
  3. filtrationwere filtered off under suction
  4. washwashed with ethanol