Acetone → HCID 53892677, compound

HRID 981866Notes

Reaction equation

HRID 981866 reaction equation
[OH-].[Na+].[CH2:3]([C:5]1[CH:12]=[CH:11][C:8]([CH:9]=O)=[CH:7][CH:6]=1)[CH3:4].[CH3:13][C:14]([CH3:16])=[O:15]>O>[CH2:3]([C:5]1[CH:12]=[CH:11][C:8]([CH:9]=[CH:13][C:14](=[O:15])[CH3:16])=[CH:7][CH:6]=1)[CH3:4]

Participants

5

Reactant 3

HCID 180AcetoneHCID 14798Sodium HydroxideHCID 208614-Ethylbenzaldehyde

Product 1

HCID 53892677HCID 53892677, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

20 ml of 10% strength sodium hydroxide solution is added to a mixture of 111.4 (0.83 mol) of 4-ethylbenzaldehyde, 133 g of acetone and 100 ml of water, and the mixture is stirred overnight at room temperature. It is then diluted with 300 ml of ice water and extracted five times, each time with 100 ml of dichloromethane. The extracts are dried over sodium sulfate and concentrated.

Workup

  1. extractionextracted five times
  2. dry with materialThe extracts are dried over sodium sulfate
  3. concentrationconcentrated

Sources & evidence

ORD record
ord-cd92bceba83e417aab24ebdade1ba423
Source dataset
uspto-grants-1991_02
Patent number
US04994106

Reaction notes

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