Methylamine → HCID 13475742, compound

Participants

Reaction Steps

The product of stage (v) (70 mg) in a saturated solution of methylamine in pyridine (4 ml) was heated at 100° in a "reactival" for 1.5 h. The mixture was concentrated and the residue oil purified by column chromatography (B) to give the title compound as an oil (7 mg), which was shown by n.m.r. and t.l.c. (B, Rf 0.3) to be identical with the product of Example 10 method (I).

Provenance & Evidence