Phosphorus oxychloride → HCID 15055713, compound
Reaction equation
O[C:2]1[C:3]2[S:14][CH2:13][CH2:12][CH2:11][C:4]=2[N:5]=[C:6]([CH2:8][O:9][CH3:10])[N:7]=1.P(Cl)(Cl)([Cl:17])=O>>[Cl:17][C:2]1[C:3]2[S:14][CH2:13][CH2:12][CH2:11][C:4]=2[N:5]=[C:6]([CH2:8][O:9][CH3:10])[N:7]=1Participants
3
Procedure
The title compound was prepared following substantially the same procedure described in Example 1, step B using the product from step B of this Example 3 and phosphorus oxychloride. This procedure gave 1.0 g of title compound which was dried and used in step D without further purification.
Workup
- customThe title compound was prepared
Sources & evidence
- ORD record
- ord-d2f43f77bf9c44e5940f095c8ddb42ac
- Source dataset
- uspto-grants-1991_02
- Patent number
- US04994464
Reaction notes
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