Phosphorus oxychloride → HCID 15055713, compound

HRID 982137Notes

Reaction equation

HRID 982137 reaction equation
O[C:2]1[C:3]2[S:14][CH2:13][CH2:12][CH2:11][C:4]=2[N:5]=[C:6]([CH2:8][O:9][CH3:10])[N:7]=1.P(Cl)(Cl)([Cl:17])=O>>[Cl:17][C:2]1[C:3]2[S:14][CH2:13][CH2:12][CH2:11][C:4]=2[N:5]=[C:6]([CH2:8][O:9][CH3:10])[N:7]=1

Participants

3

Procedure

The title compound was prepared following substantially the same procedure described in Example 1, step B using the product from step B of this Example 3 and phosphorus oxychloride. This procedure gave 1.0 g of title compound which was dried and used in step D without further purification.

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-d2f43f77bf9c44e5940f095c8ddb42ac
Source dataset
uspto-grants-1991_02
Patent number
US04994464

Reaction notes

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