HRID982204

反应详情

EQUATION

反应方程式

HRID 982204 的结构方程式

PROCEDURE

实验过程

Into a 200 cc glass reactor equipped with a reflux condenser, 50 g of 2-chloro-4,5-difluorobenzoylchloride, 13.7 g of spray dried potassium fluoride and 100 g of sulforane were charged and reacted at 135° C. for 4 hours under stirring. After cooling, the inorganic salts were filtered off, and the residue was subjected to distillation under reduced pressure to obtain 42 g of 2-chloro-4,5-difluorobenzoyl fluoride. The physical properties of the obtained 2-choloro-4,5-difluorobenzoyl fluoride were as follows.

WORKUP

后处理

  1. customInto a 200 cc glass reactor equipped with a reflux condenser
  2. customreacted at 135° C. for 4 hours
  3. temperatureAfter cooling
  4. filtrationthe inorganic salts were filtered off
  5. distillationthe residue was subjected to distillation under reduced pressure