HRID982204
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
Into a 200 cc glass reactor equipped with a reflux condenser, 50 g of 2-chloro-4,5-difluorobenzoylchloride, 13.7 g of spray dried potassium fluoride and 100 g of sulforane were charged and reacted at 135° C. for 4 hours under stirring. After cooling, the inorganic salts were filtered off, and the residue was subjected to distillation under reduced pressure to obtain 42 g of 2-chloro-4,5-difluorobenzoyl fluoride. The physical properties of the obtained 2-choloro-4,5-difluorobenzoyl fluoride were as follows.
WORKUP
后处理
- customInto a 200 cc glass reactor equipped with a reflux condenser
- customreacted at 135° C. for 4 hours
- temperatureAfter cooling
- filtrationthe inorganic salts were filtered off
- distillationthe residue was subjected to distillation under reduced pressure