HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylthiocarbamoyl chloride → HCID 20068249, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylthiocarbamoyl chloride | HCID 27871 | — |
| Reactant | HCID 14622766 | HCID 14622766 | — |
| Product | HCID 20068249 | HCID 20068249 | 93.2% |
Reaction Steps
Following the procedure described in Preparation I and starting from 27 g (0.121 mol) of 3-cyanophenyl 4-hydroxyphenyl methanone and 17.2 g (0.138 mol) of dimethylthiocarbamoyl chloride, 35 g (yield: 88%) of O-4-(3-cyanobenzoyl)phenyl dimethylthiocarbamate melting at 160° C. are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04996347 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-820dd569ecd24e68869f0b60b281c246 |
| Source note | uspto-grants-1991_02 |