HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54497776, compound → HCID 54511782, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54497776 | HCID 54497776 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54511782 | HCID 54511782 | 98.6% |
Reaction Steps
0.4 g of [N-formyl-N-benzyloxy 2(RS)-isobutyl-3-aminopropionyl]-L-leucylglycine ethyl ester in 20 ml of ethanol was hydrogenated for 0.75 hour in the presence of 5% palladium/carbon. The mixture was filtered, the filtrate was evaporated and the residue was dried in vacuo to yield 0.32 g (98%) of [N-formyl-N-hydroxy 2(RS)-isobutyl-3-aminopropionyl]-L-leucylglycine ethyl ester as a foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04996358 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-3738db60974b43a8866fb9d7bd0aa02b |
| Source note | uspto-grants-1991_02 |