HRID982969

反应详情

EQUATION

反应方程式

HRID 982969 的结构方程式

REACTANTS

反应物

2

结构：Cl

Hydrochloric Acid

ClH

结构：OC1(c2ccccc2-c2ccccc2)c2ccccc2-c2ccc(Br)cc21

未命名化合物

PRODUCTS

生成物

1

结构：Brc1ccc2c(c1)C1(c3ccccc3-c3ccccc31)c1ccccc1-2

2-Bromo-9,9'-spirobi[fluorene]

C25H15Br

AUXILIARIES

试剂、催化剂与溶剂

1

结构：CC(=O)O

Acetic Acid

C2H4O2

PROCEDURE

实验过程

47.0 g of 2-bromo-9-(biphenyl-2-yl)fluoren-9-ol were refluxed for 2.5 hours in 114 ml of 99.8% acetic acid with addition of 1.5 ml of conc. HCl.