Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3-Iodoaniline | HCID 12271 | — |
| Reactant | HCID 69732194 | HCID 69732194 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 22559497 | HCID 22559497 | 73.3% |
Reaction Steps
1 g (3.25 mmol) of 4-nitrophenyl-5-isopropyl-1,3-thiazol-2-ylcarbamate and 0.39 ml (3.25 mmol) of 3-iodoaniline were suspended under argon in 25 ml of acetonitrile. After 2 hours at 70° C. the resulting solution was cooled, giving rise 0.923 g of the title compound, recrystallized from a mixture of diethylether/pentane 1/1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06863647B2 |
|---|
| Source dataset | uspto-grants-2005_03 |
|---|
| ORD ID | ord-93ad13622d754342b5a429c586cd3a85 |
|---|
| Source note | uspto-grants-2005_03 |
|---|
