참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | 2-(N-ethylanilino)ethanol | HCID 62338 | — |
| 생성물 | Ethanol, 2-(ethylphenylamino)-, 1-acetate | HCID 113382 | — |
반응 단계
A mixture of 49.6 g (300 mmol) of 15 and 50 ml of acetic acid anhydride in a 250 ml-flask, equipped with a CaCl2-tube is stirred overnight at 60° C. Then, the volatile compounds are evaporated and the crude product is distilled under vacuüm.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06864347B2 |
|---|
| 출처 데이터셋 | uspto-grants-2005_03 |
|---|
| ORD ID | ord-6df60bb41a4a44109ff4a456fc72be8e |
|---|
| 출처 메모 | uspto-grants-2005_03 |
|---|
