HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl bromoacetate → HCID 22498599, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl bromoacetate | HCID 60984 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | 1-(3-Aminopropyl)-2-pyrrolidinone | HCID 82111 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22498599 | HCID 22498599 | — |
Reaction Steps
Methyl bromoacetate (1.35 mL, 14.3 mmol) was added dropwise to a solution of 3-aminopropyl-2-pyrrolidinone (2.0 mL, 14.3 mmol) and diisopropylethylamine (2.7 mL) in CH2Cl2. The reaction was stirred for 12 hours and was then concentrated in vacuo, and carried forward without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06867203B2 |
| Source dataset | uspto-grants-2005_03 |
| ORD ID | ord-435b55c3318248b5a337df20ddeccd8d |
| Source note | uspto-grants-2005_03 |