HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic Acid → 1-Benzoylpiperazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic Acid | HCID 243 | — |
| Reactant | tert-Butyl piperazine-1-carboxylate | HCID 143452 | — |
| Product | 1-Benzoylpiperazine | HCID 762654 | — |
Reaction Steps
This was similarly prepared from benzoic acid (5.02 g) and 1-(tert-butoxycarbonyl)piperazine (7.66 g) and the title compound was isolated as a white solid (7.7 g, 82%). LCMS: Rt 0.51 min; m/z 191 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06867192B1 |
| Source dataset | uspto-grants-2005_03 |
| ORD ID | ord-99a8681d739743e88b374893f91341f1 |
| Source note | uspto-grants-2005_03 |