HuagongsheHuagongshe Chemistry Print Report · For research reference only
o-Xylyl bromide → HCID 759632, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | o-Xylyl bromide | HCID 6992 | — |
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | 8-Chlorotheophylline | HCID 10661 | — |
| Product | HCID 759632 | HCID 759632 | — |
Reaction Steps
From 8-Chorotheophylline (10 g, 47 mmol) and 2-methylbenzyl bromide (13.6 ml, 103 mmol). The benzyl bromide was added in two portions. First half at reaction start as described in general procedure (E), and the other half after 24 hours as the reaction had not completed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06869947B2 |
| Source dataset | uspto-grants-2005_03 |
| ORD ID | ord-71293e7cd549451b8a8716f32fa2a1bf |
| Source note | uspto-grants-2005_03 |