HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyacetonitrile → HCID 20768298, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyacetonitrile | HCID 7857 | — |
| Reactant | N-BOC-ethylenediamine | HCID 187201 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20768298 | HCID 20768298 | — |
Reaction Steps
Glycolonitrile (70%, 5.10 g, 62.5 mmol), tert-butyl-N-(2-aminoethyl)carbamate (10.0 g, 62.5 mmol), and ethanol (200 mL) were combined under Ar and heated at reflux for 4 h. Removal of the solvent in vacuo gave 111 as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06870055B2 |
| Source dataset | uspto-grants-2005_03 |
| ORD ID | ord-76bdbfbc32a1462c9f069cf097528bde |
| Source note | uspto-grants-2005_03 |