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HRID985307

反应详情

EQUATION

反应方程式

HRID 985307 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[Cs+].[Cs+]
HCID10796

Cesium carbonate

CCs2O3

结构：Clc1ccnc2ccsc12
HCID11275251

7-Chlorothieno[3,2-b]pyridine

C7H4ClNS

结构：CNC(=O)c1c(C)oc2cc(O)ccc12
HCID16755173

6-Hydroxy-N,2-dimethyl-1-benzofuran-3-carboxamide

C11H11NO3

PRODUCTS

生成物

1
结构：CNC(=O)c1c(C)oc2cc(Oc3ccnc4ccsc34)ccc12
HCID20767890

N,2-Dimethyl-6-(thieno[3,2-b]pyridin-7-yloxy)-3-benzofurancarboxamide

C18H14N2O3S

PROCEDURE

实验过程

This material was prepared by the reaction of 7-chloro-thieno[3,2-b]pyridine with 6-hydroxy-2-methylbenzofuran-3-carboxylic acid methyl amide 12c and Cs2CO3 in a manner as previously described for example 1. 1H NMR (CD3CN) δ8.48 (1H, d, J=5.3 Hz), 7.91 (1H, d, J=5.6 Hz), 7.84 (1H, d, J=8.6 Hz), 7.53 (1H, d, J=5.6 Hz), 7.41 (1H, d, J=2.0 Hz), 7.20 (1H, dd, J=8.6, 2.0 Hz), 6.62 (1H, d, J=5.3 Hz), 6.60 (1H, bm), 2.91 (3H, d, J=4.6 Hz) 2.66 (3H, s).