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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 985769Generated: October 30, 2026

HCID 21917012, compound → HCID 9845508, compound

https://huagongshe.com/reaction/985769

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 21917012HCID 21917012—
SolventThionyl ChlorideHCID 24386—
ProductHCID 9845508HCID 9845508—

Reaction Conditions

Temperature60 °C

Reaction Steps

The product obtained in Step B (3 mmol), dissolved in thionyl chloride, is stirred at 60° C. under a current of nitrogen for one hour. The thionyl chloride is evaporated off under reduced pressure and the residue is dried with the aid of a vane pump to yield the title product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06872851B1
Source datasetuspto-grants-2005_03
ORD IDord-fd3582b2f9824d81a216a6449aff4b97
Source noteuspto-grants-2005_03