HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 6410643, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 2-Methoxyethylamine | HCID 8018 | — |
| Reactant | 3-Chloro-4-methyl-6-phenylpyridazine | HCID 119999 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 6410643 | HCID 6410643 | — |
Reaction Steps
A mixture of 7 g of 3-chloro 4-methyl 6-phenyl pyridazine and 7 g of 2-methoxy ethylamine in 50 ml of butanol is taken to reflux for 4 days. The hot solution is poured into 200 ml of water and extracted with ethyl acetate. The organic solution is dried over magnesium sulfate then evaporated to dryness.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04710499 |
| Source dataset | uspto-grants-1987_12 |
| ORD ID | ord-e602df8abd8e4825ae7ea9a34796eb20 |
| Source note | uspto-grants-1987_12 |