HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → HCID 51056108, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | (2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal | HCID 107526 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 51056108 | HCID 51056108 | — |
Reaction Steps
50 g of D-glucose were dissolved in 1,000 ml of hot ethanol and, after addition of 89 g of benzylamine, the mixture was left at room temperature for 48 hours. It was then cooled with ice and the product was precipitated with petroleum ether. The product was filtered off with suction, washed with ether and dried in vacuo. 1H-NMR in CD3OD: δ=7.33, broad singlet, phenyl-H.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04710491 |
| Source dataset | uspto-grants-1987_12 |
| ORD ID | ord-d3eccdd5b6754f33ba9bab80a7205778 |
| Source note | uspto-grants-1987_12 |