Water → HCID 18608593, compound

HRID 985970Notes

Reaction equation

HRID 985970 reaction equation
O=[CH:2][C@@H:3]([C@@H:5]([C@H:7]([C@H:9]([CH3:11])[OH:10])[OH:8])[OH:6])[OH:4].[CH2:12]([NH2:30])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29].O>CC(O)C>[CH2:12]([NH:30][CH:11]1[O:4][C@@H:3]([CH3:2])[C@H:5]([OH:6])[C@@H:7]([OH:8])[C@H:9]1[OH:10])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29]

Participants

5

Reactant 3

HCID 962WaterHCID 15793OctadecylamineHCID 19233(2R,3R,4S,5S)-2,3,4,5-tetrahydroxyhexanal

Product 1

HCID 18608593HCID 18608593, compound

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

9 g of L-rhamnose and 13.5 g of stearylamine were stirred in 100 ml of 2-propanol and 50 ml of water at 50° C. until a clear solution had formed. After 50 hours at room temperature, the crystals were filtered off with suction, washed with ethanol and ether and dried in vacuo.

Workup

  1. filtrationthe crystals were filtered off with suction
  2. washwashed with ethanol and ether
  3. customdried in vacuo

Sources & evidence

ORD record
ord-52f38a9c91d44569afc1d14a3c7cbf10
Source dataset
uspto-grants-1987_12
Patent number
US04710491

Reaction notes

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