HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Allylhydroxylamine hydrochloride → HCID 53692053, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Allylhydroxylamine hydrochloride | HCID 3084724 | — |
| Reactant | HCID 57075564 | HCID 57075564 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53692053 | HCID 53692053 | 53% |
Reaction Steps
1-(1,2,5,6-Tetrahydro-1-methyl-3-pyridinyl)propanone (3.06 g, 20 mmol, prepared as described in Example 8 above) was reacted with 3.27 g (30 mmol) of O-2-propenylhydroxylamine hydrochloride in 20 ml of ethanol to prepare 2.2 g (53%) of the title compound, isolated as the ethanedioate salt, mp 117°-120° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04710508 |
| Source dataset | uspto-grants-1987_12 |
| ORD ID | ord-c058afdb165f4a4ba5da25c51d2b6bf6 |
| Source note | uspto-grants-1987_12 |