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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 986030Generated: October 31, 2026

O-Allylhydroxylamine hydrochloride → HCID 53692053, compound

https://huagongshe.com/reaction/986030

Reaction equation

Participants

RoleNameHCIDCharge
ReactantO-Allylhydroxylamine hydrochlorideHCID 3084724—
ReactantHCID 57075564HCID 57075564—
SolventEthanolHCID 702—
ProductHCID 53692053HCID 5369205353%

Reaction Steps

1-(1,2,5,6-Tetrahydro-1-methyl-3-pyridinyl)propanone (3.06 g, 20 mmol, prepared as described in Example 8 above) was reacted with 3.27 g (30 mmol) of O-2-propenylhydroxylamine hydrochloride in 20 ml of ethanol to prepare 2.2 g (53%) of the title compound, isolated as the ethanedioate salt, mp 117°-120° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04710508
Source datasetuspto-grants-1987_12
ORD IDord-c058afdb165f4a4ba5da25c51d2b6bf6
Source noteuspto-grants-1987_12