HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodine → HCID 20159245, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodine | HCID 807 | — |
| Reactant | Malononitrile | HCID 8010 | — |
| Reactant | 3-(trifluoromethyl)-10H-phenothiazine | HCID 242844 | — |
| Reactant | Potassium Acetate | HCID 517044 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20159245 | HCID 20159245 | — |
Reaction Steps
To a stirred solution of 2.6 g 7-trifluoromethylphenothiazine, 1 g malononitrile and 4 g potassium acetate in 70 ml methanol was added a solution of 4 g iodine in 50 ml methanol. The precipitated dye was filtered, washed repeatedly with methanol and recrystallised in chloroform-methanol. Yield 0.6 g (18%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04710570 |
| Source dataset | uspto-grants-1987_12 |
| ORD ID | ord-d312167e654c463d93b0c996af2d0c6a |
| Source note | uspto-grants-1987_12 |