Toluene → HCID 14376313, compound

Participants

Reaction Steps

7 ml of 18% trimethylamine in toluene was added to 2.0 g (9.2 mmole) of the above tosylate, and the mixture was allowed to stand at room temperature for 3 days. The crystals separated out were collected by filtration, washed with toluene and dried under reduced pressure to give 3-hydroxypropyltrimethylammonium tosylate as colorless needles. Melting point: 80° C. Yield: 2.3 g (yield: 92%).

Provenance & Evidence