HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Toluenesulfonyl chloride → 1,5-Pentanediol monotosylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Reactant | 1,5-Pentanediol | HCID 8105 | — |
| Product | 1,5-Pentanediol monotosylate | HCID 11459578 | — |
Reaction Steps
By following a procedure of Reference Example 1, 6.2 g (60 mmole) of 1,5-pentanediol and 5.7 g (30 mmole) of tosyl chloride were treated to give 1,5-pentanediol monotosylate as a colorless oily material Yield 4.1 g (yield: 53%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04710579 |
| Source dataset | uspto-grants-1987_12 |
| ORD ID | ord-91f8b9d62de140fa8bde8c3307098ce0 |
| Source note | uspto-grants-1987_12 |