Phosphoric Acid → HCID 178446269, compound

Participants

Reaction Conditions

Reaction Steps

1.09 g of 2-phenylpentylamino-4,6-dimethyl-5-methoxypyrimidine was dissolved in 15 ml isopropylalcohol and cooled to 0° C. Phosphoric acid (85%, 9 g) was added and the mixture stirred at 0° C. for 30 minutes. White solid precipitated and was collected after removal of the isopropylalcohol, washing with pentane and drying in vacuo at 45° C. M.p.: 107°-8° C.

Provenance & Evidence