HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Nitrofurfural → 3-(6-Methoxy-3-pyridyl)-2-propenoic acid [(5-nitro-2-furyl)methylene]hydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Nitrofurfural | HCID 12774 | — |
| Reactant | 3-(6-Methoxy-3-pyridyl)-2-propenoic acid hydrazide | HCID 70435220 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-(6-Methoxy-3-pyridyl)-2-propenoic acid [(5-nitro-2-furyl)methylene]hydrazide | HCID 53796356 | — |
Reaction Steps
To a solution, heated to 50°-60° C., of 0.9 g (4.66 mmol) of 3-(6-methoxy-3-pyridyl)-2-propenoic acid hydrazide in 50 ml of methanol, 0.66g (4.7 mmol) of 5-nitrofuran-2-carbaldehyde is added.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04711892 |
| Source dataset | uspto-grants-1987_12 |
| ORD ID | ord-78e719a269844994ab187c3db866ba4a |
| Source note | uspto-grants-1987_12 |