化工社化工社 化学情報印刷レポート · 研究参考用
3'-Aminoacetophenone → 3'-Acetamidoacetophenone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3'-Aminoacetophenone | HCID 7417 | — |
| 反応物 | Acetic Anhydride | HCID 7918 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | 3'-Acetamidoacetophenone | HCID 346202 | — |
反応手順
50 ml of acetic anhydride are added in the cold to a suspension of 30 g (0.22 mole) of 1-(3-aminophenyl)ethanone in 200 ml of toluene, and the mixture is stirred for 1 h at room temperature, then heated for 1 h to 60° C. and left to stand overnight. The precipitate obtained is drained, ground in ether and dried.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04711899 |
| 出典データセット | uspto-grants-1987_12 |
| ORD ID | ord-3b778f1cd77f4826ae9e52573306c1a6 |
| 出典メモ | uspto-grants-1987_12 |