2,6-Di-tert-butyl-4-mercaptophenol → HCID 14011803, compound

HRID 986299Notes

Reaction equation

Cl[CH2:2][CH2:3][S:4]([CH2:7][C:8]([O:10][CH3:11])=[O:9])(=[O:6])=[O:5].[O-][CH2:13]C.[Na+].[CH3:16][C:17]([C:20]1[CH:25]=[C:24]([SH:26])[CH:23]=[C:22]([C:27]([CH3:30])([CH3:29])[CH3:28])[C:21]=1[OH:31])([CH3:19])[CH3:18]>>[CH3:19][C:17]([C:20]1[CH:25]=[C:24]([S:26][CH2:2][CH2:3][S:4]([CH2:7][C:8]([O:10][CH2:11][CH3:13])=[O:9])(=[O:6])=[O:5])[CH:23]=[C:22]([C:27]([CH3:30])([CH3:29])[CH3:28])[C:21]=1[OH:31])([CH3:16])[CH3:18]

Participants

Reactant 3

HCID 703702,6-Di-tert-butyl-4-mercaptophenol

HCID 2723922Sodium ethoxide

HCID 20133535HCID 20133535, compound

Product 1

HCID 14011803HCID 14011803, compound

Procedure

The title compound was prepared according to the method of Example 12 from the title compound of Example 16, sodium ethoxide and 2,6-bis(1,1-dimethylethyl)-4-mercaptophenol, m.p. ca. 95° C.

Sources & evidence

ORD record: ord-7651419618ce4c1a808f0b74d7ecf79d
Source dataset: uspto-grants-1987_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04711903

Reaction notes

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