HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thioglycolic Acid → [[2-[(2'-Hydroxy[1,1':3',1"-terphenyl]-5'-yl)thio]ethyl]thio]acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thioglycolic Acid | HCID 1133 | — |
| Reactant | 1-Bromo-2-Chloroethane | HCID 7849 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 5'-Mercapto[1,1':3',1"-terphenyl]-2'-ol | HCID 14989168 | — |
| Product | [[2-[(2'-Hydroxy[1,1':3',1"-terphenyl]-5'-yl)thio]ethyl]thio]acetic acid | HCID 14011811 | — |
Reaction Steps
The title compound was prepared according to the method of Example 13 from mercaptoacetic acid (2.3 g, 0.025 mole); 1-bromo-2-chloroethane (2.1 ml, 0.025 mole); sodium (1.8 g, 0.08 mole) and 5'-mercapto-[1,1':3',1"-terphenyl]-2'-ol (8.6 g, 0.03 mole), m.p. ca. 125° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04711903 |
| Source dataset | uspto-grants-1987_12 |
| ORD ID | ord-a2cc8d1f17f5444084a4911da313f9d7 |
| Source note | uspto-grants-1987_12 |