Benzyl 4-Hydroxybenzoate → HCID 13822732, compound

HRID 986521Notes

Reaction equation

[OH:1][C:2]1[CH:17]=[CH:16][C:5]([C:6]([O:8][CH2:9][C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)=[O:7])=[CH:4][CH:3]=1.[C:18](Cl)(=[O:22])[C:19](Cl)=[O:20]>>[CH2:9]([O:8][C:6]([C:5]1[CH:16]=[CH:17][C:2]([O:1][C:18](=[O:22])[C:19]([O:1][C:2]2[CH:3]=[CH:4][C:5]([C:6]([O:8][CH2:9][C:10]3[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=3)=[O:7])=[CH:16][CH:17]=2)=[O:20])=[CH:3][CH:4]=1)=[O:7])[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1

Participants

Reactant 2

HCID 7180Benzyl 4-Hydroxybenzoate

HCID 65578Oxalyl chloride

Product 1

HCID 13822732HCID 13822732, compound

Procedure

A similar procedure to Example 1 is carried out by using 22.8 g of benzyl p-hydroxybenzoate and 6.4 g of oxalic acid dichloride to yield di(p-benzyloxycarbonylphenyl)oxalate, m.p. 106°-108° C., as white crystals.

Sources & evidence

ORD record: ord-1f49cc29bd5e4b869a6383add8109c86
Source dataset: uspto-grants-1987_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04713474

Reaction notes

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