HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 20157948, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 20157956 | HCID 20157956 | — |
| Product | HCID 20157948 | HCID 20157948 | 99% |
Reaction Steps
Ethyl 4-[2-(1-octynyl)-phenoxy]-butanoate, (250 mg, 0.79 mmole) was hydrolysed with 1 molar equivalent of lithium hydroxide using the same procedure as in example 9. Purification of the crude material by chromatography using silica gel, eluting with chloroform to chloroform/5% methanol afforded the title compound in 99% yield as a colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04713486 |
| Source dataset | uspto-grants-1987_12 |
| ORD ID | ord-d8a1c94129ea4bdcbbfdcaa58a1a2987 |
| Source note | uspto-grants-1987_12 |